By Michael B. Smith
The Compendium of natural man made equipment sequence allows the operating chemist's look for the main worthwhile sensible staff adjustments in natural chemistry. Drawn from an exhaustive survey of the literature, Compendium of natural man made equipment, quantity 12 comprises either practical workforce changes and carbon-carbon bond-forming reactions. writer Michael Smith adheres to stringent standards for directory reactions, together with genuine artificial application and reagents which are both on hand or simply ready and dealt with within the laboratory. a transparent organizational scheme-chemical. learn more... content material: Compendium of natural artificial equipment; CONTENTS; Preface; Abbreviations; Index, Monofunctional Compounds; Index, Difunctional Compounds; advent; 1 coaching of Alkynes; 2 coaching of Acid Derivatives; three education of Alcohols; four instruction of Aldehydes; five practise of Alkyls, Methylenes, and Aryls; 6 coaching of Amides; 7 instruction of Amines; eight training of Esters; nine practise of Ethers, Epoxides, and Thioethers; 10 instruction of Halides and Sulfonates; eleven training of Hydrides; 12 training of Ketones; thirteen education of Nitriles; 14 practise of Alkenes. 15 instruction of Oxides16 education of Difunctional Compounds; writer Index. summary: The Compendium of natural artificial equipment sequence allows the operating chemist's look for the main invaluable practical team changes in natural chemistry. Drawn from an exhaustive survey of the literature, Compendium of natural artificial equipment, quantity 12 comprises either useful team changes and carbon-carbon bond-forming reactions. writer Michael Smith adheres to stringent standards for directory reactions, together with genuine man made application and reagents which are both on hand or simply ready and dealt with within the laboratory. a transparent organizational scheme-chemical
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Additional resources for Compendium of Organic Synthetic Methods -Volume 12
Lautens. ; Hiebert, S . J . Am. Chem. 2004,126,1437. ; Rao. M. Tetrahedron Lett. 2003,44,2525. SiCL, ,LiI ,BF, , 7OoC Me2HC G O Me2HC G O M e toluene/MeCN , 10h H 89% Zewee. ; King, A,; Weissman, S . ; Tschaen, D. Tetrahedron Lett. 2004,45,3729. ; Araki, S. Tetrahedron Lett. 2004,45,9189. ; Hara, H. Tetrahedron 2004,60,7973. : Li. -J. Chem. 2003,2318. BuLi ,sparteine , ether -78°C- * rt OH Y % 46% (34%ee) JIH O D 0 HO Hodnson. ; Witherington, J. Angew. Chem. Int. Ed. 2002,41,4313. H. Synlett 2002,492.
To 1. allyl-TMS ,TFS-H DCM 2 . ; Meyer, C. Synlett 2002,45. ; Osakada, K. Synlett 2002,298. / SnBu3 , aq EtOH wCHO Ph 20% Cd(C104)2/diamineligand Ph QOMe * Ph Kobayashi. ; Manabe, K. Synlett 2002,483. Io C 0 2 M 59% A , 70% ph? 4. Synlett 2002,2116. Sm (I2) ,i-PrOH PhCHO L\ L \ PhCH2OH w 96% Fukuzawa. ; Saitoh,T. Eur. J . Org. Chem. 2004,2863. / A , Zn ,NH40Ac Br PhCHO THF , 0°C Ph 91% C02Me 1. Zn , TMSCl 2. PhCHO ,NMP , 2 TMSCl * e Section 34B 85% Chen. -G. Org. Prep. Proceed. Int. 2002,34,507.
Shirakawa, S . ; Maruoka, K. Synlett 2002,575. ; Ramalingam, T . Synth. 2002,32,219. S. Synth. 2002,32,931. NaBH, , I, ,THF ,15"C F C H 94% CHZOH O 0 Singh. L. Synth. Commun. 33, 191. ; Giri. S. Synth. Commun. 2004,34,2863. ; Carretero. C. J . Org. 2002,67,1346. ; Shibasaki, M. J . Org. 2002,67,2556. Et,Zn , 10% chiral amino acid ligand hexane ,4"C 1 d PhCHO . T. J . Org. 2003,68,7509. ; Seto. T. J . Org. Chem. 2003,68,7788. PhCHO 73% (70% ee) C1,Si , B u ~ N ,I DCM ,-60°C cat chiral2,2'-bipyridyl N-oxide ,i-Pr2NEt 84% (68% ee) 85% (88% ee) Ph Malkov.